TA Instruments

Sachainchi mhumeda-0025f

27/04/2022 12:23:34 p. m.

Sample name	Sachainchi mhumeda
Sample notes	 
Experiment notes	
Operator	
Sample density	1,000 g/cm^3
Results file name	Sachainchi mhumeda
Run number	25 
Results directory	C:\Ta\Data\Ar1500\Ar1500\DIEGO ROA
Experiment was run on	27/04/2022 12:23:34 p. m.

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	25,0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:02:00 hh:mm:ss
Wait for zero velocity	No
Purge gas only	No

Step name	Stepped flow step 1
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000E-3 1/s
End controlled variable	shear rate 0,01000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 2
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,01000 1/s
End controlled variable	shear rate 0,1000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 3
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,1000 1/s
End controlled variable	shear rate 1,000 1/s
Ramp mode	log 
Points per decade	5 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 4
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000 1/s
End controlled variable	shear rate 100,0 1/s
Ramp mode	log 
Points per decade	8 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Conditioning Step 2
Step notes	
Perform step	Yes
Initial temperature	25,0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Perform pre-shear	Yes
Pre-shear variable	10,00 1/s
Pre-shear duration	0:00:10 hh:mm:ss
Motor mode	auto 
Perform equilibration	Yes
Equilibration duration	0:02:00 hh:mm:ss
Wait for zero velocity	No
Purge gas only	No

Step name	Temperature ramp step 1
Step notes	
Perform step	Yes
Ramp type	Temperature ramp
Start temperature	25,0 C
End temperature	90,0 C
Wait for start temperature	Yes
Ramp rate	10,00 C/min
Delay time	0:00:09 hh:mm:ss
Controlled variable	shear rate 10,00 1/s
Motor mode	auto 

Step name	Temperature ramp step 2
Step notes	
Perform step	Yes
Ramp type	Temperature ramp
Start temperature	90,0 C
End temperature	90,0 C
Wait for start temperature	No
Ramp duration	0:05:00 hh:mm:ss
Delay time	0:00:09 hh:mm:ss
Controlled variable	shear rate 10,00 1/s
Motor mode	auto 

Step name	Temperature ramp step 3
Step notes	
Perform step	Yes
Ramp type	Temperature ramp
Start temperature	90,0 C
End temperature	25,0 C
Wait for start temperature	No
Ramp rate	10,00 C/min
Delay time	0:00:09 hh:mm:ss
Controlled variable	shear rate 10,00 1/s
Motor mode	auto 

Step name	Conditioning Step 3
Step notes	
Perform step	Yes
Initial temperature	25,0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Perform pre-shear	Yes
Pre-shear variable	1,000 1/s
Pre-shear duration	0:00:10 hh:mm:ss
Motor mode	auto 
Perform equilibration	Yes
Equilibration duration	0:02:00 hh:mm:ss
Wait for zero velocity	No
Purge gas only	No

Step name	Stepped flow step 5
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000E-3 1/s
End controlled variable	shear rate 0,01000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 6
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,01000 1/s
End controlled variable	shear rate 0,1000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 7
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,1000 1/s
End controlled variable	shear rate 1,000 1/s
Ramp mode	log 
Points per decade	5 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 8
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000 1/s
End controlled variable	shear rate 100,0 1/s
Ramp mode	log 
Points per decade	8 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	No
Set temperature system idle	No

Geometry name	Starch cell
Geometry notes	Starch cell
Geometry material	High temperature
gap	5500 micro m
Calibration factor	10800 
Gap offset	0 micro m
Geometry inertia	2,236 micro N.m.s^2
Shear rate factor	1,000 
Shear stress factor	10800 1/m^3
Measurement system factor	10800 1/m^3
Fluid density factor	1,000E-15 m^5
Normal force factor	1,000 1/m^2
Backoff distance	1,25E5 micro m

Gap zero mode	Standard
Sample compression	none 
Compression distance	1000,0 micro m
Compression velocity	100,0 micro m/s
Fine velocity	1000,0 micro m/s
Coarse velocity	3000,0 micro m/s
Other velocity	3000,0 micro m/s
Current temperature system	Starch cell
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	5,0 C
Cooling water range	15,0 C
Bearing friction correction	Yes
Bearing friction	1,222 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1,0000 , offset 0 C
	Water bath - span 1,0000 , offset 0 C
	Torsion oven - plate - span 1,0000 , offset 0 C
	Torsion oven - solid sample - span 1,0000 , offset 0 C
	Peltier concentric cylinders - span 1,0000 , offset 0 C
	None - span 1,0000 , offset 0 C
	Stress relaxation - span 1,0000 , offset 0 C
	Current temperature system - span 1,0000 , offset 0 C
Bearing mapping type	fast 
Number of mapping iterations	1
Instrument type (MType)	AR1500ex
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	172.23.191.2
Software version	V5.8.2
Windows version	Windows XP 6.2
Instrument inertia	15,97 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0,2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0,1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	3,000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	No
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	No
Creep zero displacement	Yes
Store images to the results for creep steps	No
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	No
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	No
Flow torque limit	10,00 micro N.m
Flow velocity limit	1,000E-3 rad/s
Oscillation torque limit	5,00 micro N.m
Oscillation displacement limit	1,00E-5 rad
Oscillation raw phase limit	170,0 degrees
Oscillation minimum normal force limit	0 N
Oscillation maximum normal force limit	0 N
Flow velocity tolerance	5,00 %
Oscillation torque tolerance	1,00 %
Oscillation displacement tolerance	5,00 %
Oscillation velocity tolerance	5,00 %
Temperature tolerance	1,0 C

Stepped flow step 1

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

-3,760E-4	1,001E-3	-0,3756	9,8600	25,0	0
1,484E-3	2,153E-3	0,6895	20,000	25,0	0
4,922E-3	4,638E-3	1,061	30,079	25,0	0
0,01171	0,01000	1,170	40,110	25,0	0

Stepped flow step 2

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,01821	0,01001	1,820	9,9380	25,0	0
0,02121	0,02155	0,9846	20,063	25,0	0
0,02516	0,04641	0,5421	30,156	25,0	0
0,06574	0,1000	0,6571	40,235	25,0	0
0,04272	0,1000	0,4272	50,328	25,0	0

Stepped flow step 3

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,1424	0,09995	1,424	9,9680	25,0	0
0,06355	0,1587	0,4004	20,062	25,0	0
0,04778	0,2512	0,1902	30,187	25,0	0
0,1158	0,3984	0,2907	40,265	25,0	0
0,08226	0,6311	0,1303	50,406	25,0	0
0,06692	1,000	0,06692	60,609	25,0	0

Stepped flow step 4

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,06533	1,000	0,06530	9,9840	25,0	0
0,2503	1,334	0,1877	20,047	25,0	0
0,03467	1,778	0,01950	30,140	25,0	0
0,03229	2,371	0,01362	40,203	25,0	0
0,03919	3,162	0,01240	50,265	25,0	0
0,05446	4,217	0,01291	60,344	25,0	0
0,1015	5,624	0,01805	70,469	25,0	0
0,1714	7,499	0,02286	80,531	25,0	0
0,2967	10,00	0,02967	90,625	25,0	0
0,4460	13,33	0,03345	100,72	25,0	0
0,6357	17,78	0,03575	110,84	25,0	0
0,8903	23,71	0,03754	121,03	25,0	0
1,457	31,62	0,04607	131,16	25,0	0
2,011	42,17	0,04768	141,19	25,0	0
2,960	56,23	0,05263	151,23	25,0	0
4,771	74,99	0,06363	161,28	25,0	0
7,063	100,0	0,07063	171,36	25,0	0

Temperature ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,1721	10,00	0,01721	9,0040	25,0	0
0,1721	10,00	0,01721	17,988	25,4	0
0,1689	10,00	0,01689	27,004	26,5	0
0,1906	9,996	0,01907	35,996	28,0	0
0,1729	10,00	0,01729	44,996	29,7	0
0,1773	9,999	0,01773	54,000	31,5	0
0,1585	10,00	0,01584	62,988	33,2	0
0,1658	9,999	0,01658	71,992	35,0	0
0,1567	10,00	0,01567	80,996	36,6	0
0,1619	10,00	0,01619	90,000	38,2	0
0,1571	9,999	0,01571	99,008	39,8	0
0,1714	9,998	0,01714	108,00	41,3	0
0,1493	10,00	0,01493	117,01	42,9	0
0,1542	10,00	0,01542	126,00	44,3	0
0,1704	9,999	0,01705	135,00	45,9	0
0,1436	10,00	0,01436	143,99	47,4	0
0,1415	10,00	0,01415	152,99	48,8	0
0,1427	10,00	0,01427	161,99	50,3	0
0,1415	10,00	0,01415	170,99	51,9	0
0,1389	10,00	0,01389	179,99	53,3	0
0,1514	9,999	0,01514	188,99	54,8	0
0,1227	10,01	0,01226	198,00	56,3	0
0,1394	10,00	0,01394	207,00	57,8	0
0,1322	10,00	0,01322	216,00	59,3	0
0,1447	9,998	0,01447	224,99	60,8	0
0,1409	10,00	0,01409	233,99	62,3	0
0,1395	10,00	0,01395	243,00	63,8	0
0,1364	10,01	0,01363	252,00	65,3	0
0,1427	10,00	0,01427	261,01	66,8	0
0,1380	10,00	0,01380	269,99	68,3	0
0,1512	10,00	0,01512	278,99	69,8	0
0,1494	10,00	0,01494	288,01	71,2	0
0,1767	10,00	0,01767	297,00	72,8	0
0,2117	10,00	0,02117	306,00	74,4	0
0,2323	10,00	0,02323	315,00	75,8	0
0,3655	9,999	0,03656	323,98	77,2	0
0,5959	10,00	0,05960	332,99	78,6	0
0,7771	10,00	0,07771	342,00	80,2	0
0,7216	10,00	0,07216	350,99	81,9	0
0,4812	9,999	0,04812	359,99	83,7	0
0,4160	10,00	0,04160	369,00	85,3	0

Temperature ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,4216	9,998	0,04217	8,9960	87,1	0
0,4150	9,999	0,04150	17,992	89,3	0
0,4453	10,00	0,04453	26,992	90,8	0
0,5158	9,999	0,05159	35,992	91,7	0
0,3530	9,999	0,03531	44,988	91,6	0
0,3100	10,00	0,03100	53,996	90,1	0
0,3167	9,999	0,03167	62,992	89,7	0
0,3001	9,999	0,03001	72,000	89,8	0
0,2695	10,00	0,02695	80,992	90,1	0
0,2740	10,00	0,02740	90,004	90,3	0
0,2495	10,00	0,02495	98,996	90,5	0
0,2471	10,00	0,02471	107,99	90,6	0
0,2623	10,00	0,02623	117,00	90,6	0
0,2485	10,00	0,02485	126,01	90,6	0
0,2467	10,00	0,02467	134,98	90,5	0
0,2532	10,00	0,02532	144,00	90,4	0
0,2448	10,00	0,02448	152,99	90,3	0
0,4488	9,998	0,04489	162,00	90,2	0
0,2630	10,00	0,02630	170,99	90,1	0
0,2803	9,995	0,02804	179,99	90,1	0
0,2600	9,999	0,02600	189,00	90,1	0
0,2517	10,00	0,02517	198,00	90,1	0
0,2606	10,00	0,02606	207,00	90,1	0
0,2684	10,00	0,02684	216,01	90,0	0
0,2459	10,00	0,02458	224,99	90,0	0
0,2514	10,00	0,02513	233,99	90,0	0
0,2638	9,999	0,02639	243,00	90,0	0
0,3603	10,00	0,03603	251,99	90,0	0
0,2460	9,999	0,02460	260,99	90,0	0
0,2511	10,00	0,02511	269,99	90,0	0
0,2475	10,00	0,02475	279,00	90,0	0

Temperature ramp step 3

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,2629	10,00	0,02629	9,0120	90,0	0
0,2621	9,999	0,02621	18,004	89,3	0
0,2673	10,00	0,02673	27,008	87,2	0
0,2892	10,00	0,02892	36,000	86,0	0
0,2833	10,00	0,02833	45,008	84,8	0
0,2941	10,00	0,02941	54,008	83,0	0
0,3012	10,00	0,03012	63,024	81,5	0
0,3009	9,999	0,03009	72,012	80,1	0
0,3589	9,983	0,03595	81,008	78,2	0
0,2998	9,999	0,02998	90,004	76,9	0
0,3290	9,999	0,03291	99,004	75,2	0
0,3217	10,00	0,03217	108,02	73,8	0
0,3171	10,00	0,03170	117,01	72,2	0
0,3285	10,00	0,03286	126,01	70,6	0
0,3228	10,00	0,03228	135,00	69,3	0
0,3436	10,00	0,03436	144,00	67,6	0
0,3270	9,999	0,03271	153,02	66,3	0
0,3691	10,00	0,03691	162,01	64,6	0
0,3435	10,00	0,03435	171,02	63,2	0
0,3355	10,00	0,03355	180,00	61,6	0
0,3553	9,998	0,03554	189,01	60,1	0
0,3666	9,999	0,03666	198,01	58,7	0
0,3613	10,00	0,03613	206,99	57,2	0
0,3702	10,00	0,03702	216,01	55,7	0
0,4003	9,998	0,04004	225,01	54,2	0
0,3844	9,999	0,03845	234,01	52,7	0
0,4069	10,00	0,04069	243,00	51,2	0
0,4035	10,00	0,04035	252,00	49,8	0
0,4070	10,01	0,04068	261,01	48,3	0
0,4092	10,00	0,04092	270,00	46,7	0
0,4181	10,00	0,04181	279,01	45,2	0
0,4395	9,999	0,04395	288,00	43,7	0
0,4433	9,999	0,04433	297,00	42,2	0
0,4919	10,00	0,04919	306,01	40,8	0
0,4395	10,00	0,04395	315,00	39,3	0
0,4649	9,999	0,04650	324,01	37,7	0
0,4730	10,00	0,04729	333,00	36,2	0
0,4623	10,00	0,04623	342,00	34,8	0
0,4958	9,999	0,04959	351,00	33,3	0
0,4658	10,00	0,04657	360,01	31,8	0
0,4931	9,999	0,04931	369,00	30,4	0

Stepped flow step 5

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,01507	9,956E-4	15,13	9,9370	25,0	0
0,03662	2,151E-3	17,03	20,031	25,0	0
0,1135	4,638E-3	24,47	30,140	24,9	0
0,3854	9,997E-3	38,56	40,234	25,0	0

Stepped flow step 6

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,7297	9,997E-3	72,99	9,9530	25,0	0
1,050	0,02154	48,76	20,015	25,0	0
1,478	0,04641	31,85	30,093	25,0	0
2,213	0,1000	22,12	40,453	24,9	0
1,904	0,1000	19,04	50,515	25,0	0

Stepped flow step 7

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

1,753	0,09999	17,54	9,9840	25,0	0
1,973	0,1585	12,45	20,063	25,0	0
2,159	0,2511	8,598	30,141	25,0	0
1,602	0,3980	4,025	40,203	25,0	0
1,456	0,6307	2,308	50,219	25,0	0
1,091	0,9998	1,091	60,297	25,0	0

Stepped flow step 8

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

1,070	1,000	1,070	9,9690	25,0	0
0,9027	1,333	0,6773	20,016	25,0	0
0,7303	1,779	0,4106	30,125	25,0	0
0,5847	2,372	0,2465	40,219	25,0	0
0,4232	3,162	0,1338	50,344	25,0	0
0,4629	4,216	0,1098	60,375	25,0	0
0,3855	5,623	0,06855	70,453	25,0	0
0,4559	7,499	0,06080	80,500	25,0	0
0,5153	10,00	0,05153	90,547	25,0	0
0,7432	13,34	0,05573	100,61	25,0	0
1,128	17,78	0,06345	110,69	25,0	0
2,674	23,71	0,1128	120,78	25,0	0
3,112	31,62	0,09840	130,84	25,0	0
3,960	42,17	0,09391	140,94	25,0	0
5,701	56,24	0,1014	151,00	25,0	0
7,914	74,99	0,1055	161,06	25,0	0
10,54	100,0	0,1054	171,14	25,0	0

